Van der Waals Clathrates (Bipy)3·(SO2)·(H2O), (Bipy)2·(SO2)·(H2O)2 and (Bz3N)3·(SO2)

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dc.contributor.authorKhoma, Ruslan E. en
dc.contributor.authorGelmboldt, V. O.en
dc.contributor.authorEnnan, Alim-Abdul A.en
dc.contributor.authorBaumer, Vyacheslav N.en
dc.contributor.authorХома, Руслан Євгенійовичuk
dc.date.accessioned2018-02-13T09:12:11Z
dc.date.available2018-02-13T09:12:11Z
dc.date.issued2017
dc.description.abstractReaction products have been isolated from “sulphur dioxide – 2,2′-bipyridine – water” and “sulphur dioxide – tribenzylamine – water – benzene” systems. Crystallization of 2,2′- bipyridine from aqueous solution containing sulfur(IV) oxide afforded clathrates with the compositions (bipy)3·(SO2)·(H2O) (1) and (bipy)2·(SO2)·(H2O)2 (2) [1]. X-Ray amorphous guest SO2 molecules occupy voids in the crystal lattice of 2,2′-bipyridine without distortion of its structure. Van der Waals clathrate with the composition (Bz3N)3·(SO2) (3) was obtained for tribenzylamine. Only starting Bz3N was obtained from “sulphur dioxide – tribenzylamine – water – benzene” system. The isolated compounds were characterized by elemental analyses, X-ray diffraction data, and IR, NMR, and mass spectra.en
dc.identifier.citation27th International Chugaev Conference on Coordination Chemistry (October 2–6, 2017, Nizhny Novgorod)uk
dc.identifier.urihttps://dspace.onu.edu.ua/handle/123456789/12780
dc.language.isoen
dc.subjectVan der Waals clathrateen
dc.subjectsulphur dioxideen
dc.subjecttribenzylamineen
dc.titleVan der Waals Clathrates (Bipy)3·(SO2)·(H2O), (Bipy)2·(SO2)·(H2O)2 and (Bz3N)3·(SO2)en
dc.typeArticle
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